Protocol | Description | Duration [min] | References |
---|---|---|---|
1 | 0,3°C/min to −100°C | 347 |  |
 | Store in vapour phase at −134°C |  | [47]* |
2 | 1°C/min to −80°C | 84 | |
 | Store in vapour phase at −134°C |  |  |
3 | 1°C/min to - 30°C | 44 |  |
 | 5°C/min to −80°C |  | |
 | xStore in vapour phase at −134°C |  |  |
4 | 1°C/min to −20°C | 34 |  |
 | 5°C/min to −40°C |  |  |
 | 10°C/min to −80°C |  | Designed |
 | 20°C/min to −100°C |  |  |
 | Store in vapour phase at −134°C |  |  |
5 | 1°C/min to −6°C | 26 |  |
 | 25°C/min to −50°C |  | Designed |
 | 10°C/min to −90°C |  |  |
 | Store in vapour phase at −134°C |  |  |
6 | Directly into the vapour phase | 0 | Â |
7 | 99°C/min to −100°C | 2 |  |
 | Store in vapour phase at −134°C |  |